Journal of Siberian Federal University. Chemistry: Effect of the Mechanical and Thermal Prehistory of Precursors on the Zinc Spinel Synthesis

Journal of Siberian Federal University. Chemistry / Effect of the Mechanical and Thermal Prehistory of Precursors on the Zinc Spinel Synthesis

Issue: Journal of Siberian Federal University. Chemistry. 2020 13 (1)
Authors: Kosenko, Nadezhda F.; Filatova, Natalya V.; Rodionova, Viktoriia I.
Contact information: Kosenko, Nadezhda F.: Ivanovo State University of Chemistry and Technology Ivanovo, Russian Federation; Filatova, Natalya V.: Ivanovo State University of Chemistry and Technology Ivanovo, Russian Federation; ; Rodionova, Viktoriia I.: Ivanovo State University of Chemistry and Technology Ivanovo, Russian Federation
Keywords: zinc spinel; gahnite; solid-phase synthesis; mechanical activation; microwave treatment
Abstract: Thezinc spinel (gahnite) formation by a treatment of reaction mixtures of Zn and Al oxides, hydroxides, and salts was investigated. The influence of a preliminary mechanical activation by impact (planetary mill) and attrition (ball-ring mill) action as well as a microwave treatment was analyzed. The combined method consisting of a mechanical treatment of nitrates mixture in a planetary mill and the subsequent burning in a thermal kiln was considered as the most effective as it resulted in practically single product
Pages: 53-64
DOI: 10.17516/1998-2836-0168
Paper at repository of SibFU: https://elib.sfu-kras.ru/handle/2311/135083