Journal of Siberian Federal University. Chemistry / Development of Methods for Phenols Determination in Drink and Natural Water Using Capillary Electrophoresis and High Performance Liquid Chromatography

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Issue
Journal of Siberian Federal University. Chemistry. 2010 3 (3)
Authors
Sursyakova, Viktoriya V.; Burmakina, Galina V.; Rubaylo, Anatoliy I.
Contact information
Сурсякова, В.В. : Институт химии и химической технологии СО РАН , Россия 660049, Красноярск, ул. К. Маркса, 42 , e-mail: ; Бурмакина, Г.В. : Институт химии и химической технологии СО РАН Сибирский федеральный университет , Россия 660049, Красноярск, ул. К. Маркса, 42 Россия 660041, Красноярск, пр. Свободный, 79; Рубайло, А.И. : Институт химии и химической технологии СО РАН Сибирский федеральный университет , Россия 660049, Красноярск, ул. К. Маркса, 42 Россия 660041, Красноярск, пр. Свободный, 79; Sursyakova, Viktoriya V. : Institute of Chemistry and Chemical Technology, Siberian Branch of the Russian Academy of Sciences , 42 К. Marks st., Krasnoyarsk, 660049 Russia , e-mail: ; Burmakina, Galina V. : Institute of Chemistry and Chemical Technology, Siberian Branch of the Russian Academy of Sciences Siberian Federal University , 42 К. Marks st., Krasnoyarsk, 660049 Russia 79 Svobodny, Krasnoyarsk, 660041 Russia; Rubaylo, Anatoliy I. : Institute of Chemistry and Chemical Technology, Siberian Branch of the Russian Academy of Sciences Siberian Federal University , 42 К. Marks st., Krasnoyarsk, 660049 Russia 79 Svobodny, Krasnoyarsk, 660041 Russia
Keywords
phenols; chlorophenols; drink water; natural water; capillary electrophoresis; high performance liquid chromatography
Abstract

The methods for phenols determination in drink and natural water using capillary electrophoresis (CE) and high performance liquid chromatography (HPLC) were developed. The detection limits without pre-concentration are 0,2-0,5 mg/l for CE and 0,02-0,05 mg/l for HPLC. The detection limits with pre-concentration by solid-phase exctraction using cartridge DIAPAK P («BioChemMac ST») were high per thousand. It is allows to determine phenols with content at 0,5 of maximum allowable concentration (MAC) and below it.

Pages
268-277
Paper at repository of SibFU
https://elib.sfu-kras.ru/handle/2311/2185