Journal of Siberian Federal University. Chemistry / Chromatography-Mass Spectrometry Determination Some of the Female Sex Hormones that Have the Steroid Structure and their Synthetic Analogues

Full text (.pdf)
Issue
Journal of Siberian Federal University. Chemistry. 2010 3 (4)
Authors
Sokolova, Lidia S.; Strukova, Elena S.; Dukova, Olga A.
Contact information
Sokolova, Lidia S. : Siberian Federal University , 79 Svobodny, Krasnoyarsk, 660041 Russia; Strukova, Elena S. : Siberian Federal University , 79 Svobodny, Krasnoyarsk, 660041 Russia; Dukova, Olga A. : Siberian Federal University , 79 Svobodny, Krasnoyarsk, 660041 Russia
Keywords
BSTFA; female sex hormones steroid structure; gas chromatography-mass spectrometry; derivatized; BSTFA
Abstract

It was shown the possibility of qualitative and quantitative determination of some of the female sex steroid hormones and their analogues in the form of methyl esters by the method of chromatographymass spectrometry. It was calculated detection limits of investigated steroid hormones and their methyl esters using the method of gas chromatography-mass spectrometry. Found that after the derivatizations reaction the limit of quantification of these substances is reduced on average by 3 times.

Pages
408-412
Paper at repository of SibFU
https://elib.sfu-kras.ru/handle/2311/2317