Siberian Federal University 
- Issue
- Journal of Siberian Federal University. Chemistry. 2014 7 (1)
- Authors
- Komar, Natalia A.; Slaschinin, Dimitri G.; Peterson, Ivan V.; Tovbis, Mikhail S.
- Contact information
- Komar, Natalia A.:Siberian State Technological University, 82 Mira, Krasnoyarsk, 660049 Russia; Slaschinin, Dimitri G.:Siberian State Technological University, 82 Mira, Krasnoyarsk, 660049 Russia; Peterson, Ivan V.:Institute of Chemistry and Chemical Technology Siberian Branch of the Russian Academy of Sciences 50/24 Akademgorodok, Krasnoyarsk, 660036 Russia; Tovbis, Mikhail S.:Siberian State Technological University, 82 Mira, Krasnoyarsk, 660049 Russia
- Keywords
- arylamides; cyclization; persubstituted nitrosophenols; isophtalic acid; NMR spectroscopy; tautomerism
- Abstract
The cyclization of arylamides acetonedicarboxylate with isonitrosoacetylacetone was carried out. Arylamides of potassium salts of 2-hydroxy-5-nitroso-4,6- dimethylisophtalic acid were synthesized and characterized. Relevant nitrosophenols in a free form were preparated from these salts and their properties were investigated. 1H NMR spectroscopy showed that DMSO-d6 solutions of these compounds are entirely in the oxime form
- Pages
- 36-41
- Paper at repository of SibFU
- https://elib.sfu-kras.ru/handle/2311/10271
Journal of Siberian Federal University. Chemistry / Preparation and Properties of new Arylamides of 2-Hydroxy-5-Nitroso-4,6-Dimethylisophtalic Acid
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